View information & documentation regarding Oxalyl chloride, including CAS, MSDS & more. <>
Oxalyl chloride is a chemical compound with the formula (COCl)2. It is toxic by inhalation, although it is over an order of magnitude less acutely toxic than the related compound phosgene. [14] It is toxic by inhalation, although it is over an order of magnitude less acutely toxic than the related compound phosgene. Oxalyl chloride is mainly used as a catalyst in the oxidation of alcohols to the corresponding aldehydes and ketones. Chemical Formula: (ClCO)2 Contact Information: Finar Limited 184-186/P, Chacharwadi Vasna, This colourless, sharp-smelling liquid, the diacyl chloride of oxalic acid, is a useful reagent in organic synthesis. [10] Relative to thionyl chloride, oxalyl chloride tends to be a milder, more selective reagent. X���`I�%&/m�{J�J��t��`$ؐ@������iG#)�*��eVe]f@�흼��{���{���;�N'���?\fdl��J�ɞ!���?~|? Skin Contact Wash off immediately with plenty of water for at least 15 minutes. Oxalyl chloride reacts with aromatic compounds in the presence of aluminium chloride to give the corresponding acyl chloride in a process known as a Friedel-Crafts acylation. oxalyl chloride msds sold here are of the highest quality. 5.3. One of the minor byproducts from the N,N-dimethylformamide catalyzed reaction is a potent carcinogen, stemming from the N,N-dimethylformamide decomposition. Oxalylchloride is een organische verbinding met als brutoformule C2O2Cl2. Oxalyl Chloride: Oxalyl Chloride: 79-37-8: none: European Inventory of Existing Commercial Chemical Substances (EINECS) Listed. Constituent 1. It is actively used for the synthesis of acid chlorides from acids. The solution comprising DMSO and oxalyl chloride, followed by quenching with triethylamine converts alcohols to the corresponding aldehydes and ketones via the process known as the Swern oxidation.[7][8][9]. Inhalation If not breathing, give artificial respiration. Shop a large selection of Acyl halides products and learn more about Oxalyl chloride, 98%, ACROS Organics. Transport information DOT UN-No UN3130 Proper Shipping Name WATER-REACTIVE LIQUID, TOXIC, N.O.S. The diester derived from phenol, phenyl oxalate ester, is Cyalume, the active ingredient in glow sticks. It is also more expensive than thionyl chloride so it tends to be used on a smaller scale. Oxalyl chloride Revision Date 23-May-2017 14. In this, it is quite different from other acyl chlorides which hydrolyze with formation of hydrogen chloride and the original carboxylic acid. United States Toxic Substances Control Act (TSCA) Inventory: Listed. "R}~Q:~pgg'������"���l���/���������O�:OϽV�ޞ�~
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Display Name: Oxalyl dichloride EC Number: 201-200-2 EC Name: Oxalyl dichloride ... OXALYL CHLORIDE . endobj
NFPA SUPPLIER Company: Santa Cruz Biotechnology, Inc. 2145 Delaware Ave … Pick your sack of pure, reliable, and hot-selling oxalyl chloride msds solutions at Alibaba.com at some splendid deals. - Find MSDS or SDS, a COA, data sheets and more information. Chemsrc provides Oxalyl chloride(CAS#:79-37-8) MSDS, density, melting point, boiling point, structure, formula, molecular weight etc. View or download the Oxalyl chloride MSDS (Material Safety Data Sheet) or SDS for 807066 from Merck. >>
Methyl oxalyl chloride Revision Date 18-Jan-2018 Conditions to Avoid Exposure to moist air or water. Use only under a chemical fume hood. Aldrich-O8801; Oxalyl chloride reagent grade, 98%; CAS No. [3], Oxalyl chloride was first prepared in 1892 by the French chemist Adrien Fauconnier, who reacted diethyl oxalate with phosphorus pentachloride. It is actively used for the synthesis of acid chlorides from acids. : 79-37-8 1.2 Relevant identifi ed uses of the substance or mixture and uses advised against Identified uses : Laboratory chemicals, Manufacture of substances 1.3 Details of the supplier of the safety data sheet Company : Sigma-Aldrich 3050 Spruce Street Keep away from open flames, hot surfaces and sources of ignition. [13], In March 2000, a Malaysia Airlines Airbus A330-300 was damaged beyond repair after a cargo of prohibited oxalyl chloride (falsely declared as hydroxyquinoline) leaked into the cargo bay. Oxalyl chloride MSDS Section 1: Chemical Product and Company Identification Product Name: Oxalyl chloride Catalog Codes: 11084 CAS#: 79-37-8 RTECS: Not available. In the Fridel-Crafts acylation reaction, it reacts with aromatic compounds to get the corresponding acyl choride using aluminum chloride as catalyst. Oxalylchloride is een veelgebruikt reagens in de organische synthese. Handling, Storage, and Precautions: (see also Oxalyl Chloride ); reagent generated in situ under anhydrous conditions; corrosive, toxic. CAS 79-37-8, EC Number 201-200-2, chemical formula ClCOCOCl. Application Oxalyl chloride may be used in the following processes: • Preparation of Mosher′s acid chloride by reacting with Mosher′s acid in the presence of DMF. Oxalyl chloride reacts with water giving off gaseous products only: hydrogen chloride (HCl), carbon dioxide (CO2), and carbon monoxide (CO). TSCA: TSCA 8(b) inventory: Oxalyl chloride CI#: Not available. Safety Data Sheet (Oxalyl Chloride) DATE PREPARED: 2/10/2016 Page 5 of 6 Carcinogenicity: The components of this product are not listed as carcinogen by ACGIH, IARC, NIOSH, NTP, or OSHA. ;�j`�&
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��������������y���}�����1|��O� ~xpOlC8�y���u�P[�NnL�7�8�a'��|]\7�B8a���=�Η�WC�:�����v��3�Nx��b�X�zC�6�k3#�o���sۜs���i��q�m����������SG\:vf�þ�! Oxalyl chloride for synthesis. Oxalyl chloride sc-215640 Hazard Alert Code Key: EXTREME HIGH MODERATE LOW Section 1 - CHEMICAL PRODUCT AND COMPANY IDENTIFICATION PRODUCT NAME Oxalyl chloride STATEMENT OF HAZARDOUS NATURE CONSIDERED A HAZARDOUS SUBSTANCE ACCORDING TO OSHA 29 CFR 1910.1200. This reaction involves conversion of DMF to the imidoyl chloride derivative (Me2N=CHCl+), akin to the first stage in the Vilsmeier–Haack reaction. [11][12] The resulting acyl chloride can be hydrolysed to form the corresponding carboxylic acid. MSDS Name: Methyl Oxalyl Chloride, 97% Catalog Numbers: AC166000000, AC166000250 Synonyms: Methyl Chloroglyoxylate. OXALYL CHLORIDE CAS No 79-37-8 MATERIAL SAFETY DATA SHEET SDS/MSDS SECTION 1: Identification of the substance/mixture and of the company/undertaking 1.1 Product identifiers Product name : Oxalyl Chloride CAS-No. Min.Order: 1 Metric Ton FOB Price: USD $ 1.0-3.0/Metric Ton hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm Oxalyl chloride Revision Date 20-Feb-2019 Hazardous Combustion Products Hydrogen chloride gas, Carbon monoxide (CO), Carbon dioxide (CO2), Phosgene. [5], Oxalyl chloride is produced commercially from ethylene carbonate. Het kan beschouwd worden als het diacylchloride van oxaalzuur. Oxalic acid undergoes many of the reactions characteristic of other carboxylic acids. CAS 79-37-8, EC Number 201-200-2, chemical formula ClCOCOCl. Immediate medical attention is required. Substance identity Substance identity. Do not breathe mist/vapors/spray. [�ą/�&g��P;���C��O��w+h�a���1�$j'���a�N7�o;�=�i�dt��}���_�
��ݽ������� �ƍǀ^��Мw|��o�~��ݧ�Ȁ����-xtV�����2+��V���a�K F?x�>�fˋ�� �!�#o�?X͚�� In March 2000, a Malaysia Airlines Airbus A330-300 was damaged beyond repair after a cargo of prohibited oxalyl chloride (falsely declared as hydroxyquinoline) leaked into the cargo bay. 各製品詳細ページ，製品書類検索で分析チャートが検索できるようになりました。 (ご提供している分析チャートの種類は製品ごとに異なります。) ｜ tciメール最新号no.185を公開しました。 ｜ 弊社ウェブサイトにおける不具合について Product name : Oxalyl chloride Product Number : 75760 Brand : Aldrich CAS-No. Oxalyl chloride CAS NO.79-37-8. /Producer(Sub Systems, Inc.)/CreationDate(D:20200302051951+05'00')/ModDate(D:20200302051951+05'00')/Creator(Sub Systems, Inc.)
Hazardous Reactions Reacts violently with water. Like other acyl chlorides, oxalyl chloride reacts with alcohols to give esters: Typically, such reactions are conducted in the presence of a base such as pyridine. It forms esters such as dimethyl oxalate (m.p. chemBlink provides samples of SDS, Safety Data Sheets, for Oxalyl chloride, CAS 79-37-8 Oxalyl chloride is a commonly used chlorinating reagent that can be prepared by the reaction of oxalic acid and phosphorus pentachloride. Synonym: Chemical Name: Not available. : 79-37-8; Synonyms: Ethanedioyl dichloride; Linear Formula: ClCOCOCl; Empirical Formula: C2Cl2O2; find related products, papers, technical documents, MSDS & more at Sigma-Aldrich. Sigma-Aldrich offers a number of Oxalyl chloride products. stream
De zuivere stof komt voor als een kleurloze vloeistof met een indringende geur, die hevig reageert met water en daarbij het giftige waterstofchloride vrijstelt. Advice for firefighters As in any fire, wear self-contained breathing apparatus pressure-demand, MSHA/NIOSH (approved or … Oxalyl chloride is mainly used as a catalyst in the oxidation of alcohols to the corresponding aldehydes and ketones. %PDF-1.4
Oxalyl chloride SDS details show. China Catalog of Hazardous chemicals 2015: Listed. It forms an acid chloride called oxalyl chloride.. Oxalate, the conjugate base of oxalic acid, is an excellent ligand for metal ions, e.g. ��)�j&�Qm8�ẽ_���)z�s�ς�nT��� m��!��i��U8áy��3l��ц�"%j�nt�B���e�Ћ���b��ja��>6;q�|���u����@;3ؙ�16F!��T�ހP�eg�����vRd6� ����>�B�oTO=�e��3��(��m|��. Special Remarks on Toxicity to Animals: No data available Special Remarks on Chronic Effects on Humans: No data available Special Remarks on other Toxic Effects on Humans: No data available Do not ingest. If swallowed then seek immediate medical assistance. Contact Persons responsible for the SDS; Identification. Articles of Oxalyl chloride are included as well. New Zealand Inventory of Chemicals (NZIoC) Listed. CAS: 79-37-8 MDL: MFCD00000704 EINECS: 201-200-2 Synonyms: Oxalyl chloride Hazard Class 4.3 Subsidiary Hazard Class8, 6.1 Packing Group II IATA We provide Oxalyl chloride safety data sheets view and download at Echemi.com. Type: legal entity composition of the substance State Form: liquid. %����
25g; Glass bottle. Hazard Class 4.3 Subsidiary Hazard Class8, 6.1 Packing Group II TDG UN-No UN3130 Proper Shipping Name WATER-REACTIVE LIQUID, TOXIC, N.O.S. Oxalyl chloride, 2.0M solution in dichloromethane Revision Date 28-Nov-2019 7. 4 0 obj
Incompatible Materials Strong oxidizing agents Hazardous Decomposition ProductsCarbon monoxide (CO), Carbon dioxide (CO2) Hazardous Polymerization No information available. Oxalyl chloride was reportedly used in the first synthesis of dioxane tetraketone (C4O6), an oxide of carbon. EC Inventory: Listed. Photochlorination gives the tetrachloride, which is subsequently degraded:[6]. 1 0 obj
The intermediate dimethylforminium chloride (DMFCl) can be isolated as a hygroscopic solid, mp 140 °C (see also Thionyl Chloride, Phosphorus Oxychloride). The substance identifiers displayed in the InfoCard are the best available substance name, EC number, CAS number and/or the … [4] It can also be prepared by treating oxalic acid with phosphorus pentachloride. : 79-37-8 1.2 Relevant identified uses of the substance or mixture and uses advised against Ethyl oxalyl chloride ~95%; EC Number: 225-285-0; Synonym: Ethyl chloroglyoxylate; find Sigma-Aldrich-E6503 MSDS, related peer-reviewed papers, technical documents, similar products & more at … Oxalyl chloride is mainly used together with a N,N-dimethylformamide catalyst in organic synthesis for the preparation of acyl chlorides from the corresponding carboxylic acids. 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Oxalyl chloride Revision Date 18-Jan-2018 Conditions to Avoid Exposure to air. The reagent degrades into volatile side products in this, it is used... Different from other acyl chlorides which hydrolyze with formation of hydrogen chloride and original... Reaction, it reacts with aromatic compounds to get the corresponding acyl choride aluminum! 15 minutes acyl chlorides which hydrolyze with formation of hydrogen chloride and the original carboxylic acid of less., toxic, N.O.S aromatic compounds to get the corresponding acyl choride using aluminum chloride as.. ( CO2 ) Hazardous Polymerization No information available phosphorus pentachloride although it is quite from! Oxalic acid undergoes many of the minor byproducts from the N, Decomposition... And learn more about Oxalyl chloride MSDS ( Material Safety data sheets and information! - Find MSDS or SDS for 807066 from Merck corresponding carboxylic acid ] Relative to thionyl chloride, Oxalyl tends... And more information chloride product Number: 75760 Brand: Aldrich CAS-No TSCA: 8... Information available EC Number: 201-200-2 EC Name: Oxalyl chloride MSDS sold here are of the reactions of... Byproducts from the N, N-dimethylformamide Decomposition chloride, 98 %, Acros Organics one of the byproducts. Ec Name: Oxalyl chloride, the reagent degrades into volatile side products in this,... B ) Inventory: Oxalyl chloride CI #: Not available oxalate ester, Cyalume... Active ingredient in glow sticks is subsequently degraded: [ 6 ] N, Decomposition! Carboxylic acids MSDS ( Material Safety data sheets view and download at Echemi.com een organische verbinding met als brutoformule.... Chloride can be hydrolysed to Form the corresponding aldehydes and ketones on clothing download the Oxalyl chloride for synthesis (. Of the highest quality it tends to be a milder, more selective reagent EC Number 201-200-2, formula! Chloride is a potent carcinogen, stemming from the N, N-dimethylformamide catalyzed reaction is a compound. State Form: LIQUID from substance Identification information from all ECHA databases about Oxalyl chloride synthesis... To Form the corresponding acyl choride using aluminum chloride as catalyst more reagent... 5 ], Oxalyl chloride is mainly used as a catalyst in the oxidation of alcohols the... This application, which simplifies workup agents Hazardous Decomposition ProductsCarbon monoxide ( CO ), oxide... Treating oxalic acid undergoes many of the highest quality: 201-200-2 EC Name: Oxalyl.... 11 ] [ 12 ] the resulting acyl chloride can be hydrolysed to Form the corresponding carboxylic acid acids... In organic synthesis is actively used for the synthesis of dioxane tetraketone C4O6! Documentation regarding Oxalyl chloride for synthesis °C ( 126.5 to 128.3 °F ) ) used on a smaller.. More selective reagent handling and storage handling Wear personal protective equipment/face protection acyl choride using chloride! 4 ] it can also be prepared by treating oxalic acid, is Cyalume, the diacyl of! At least 15 minutes to moist air or water cas, MSDS & more synthesis. States toxic Substances Control Act ( TSCA ) Inventory: Oxalyl chloride Safety data sheets more! Control Act ( TSCA ) Inventory: Oxalyl dichloride... Oxalyl chloride MSDS Material. The Oxalyl chloride Safety data Sheet ) or SDS, a COA, data and. A potent carcinogen, stemming from the N, N-dimethylformamide Decomposition hydrolyze with formation of hydrogen chloride and original. ( ご提供している分析チャートの種類は製品ごとに異なります。 ) ｜ tciメール最新号no.185を公開しました。 ｜ 弊社ウェブサイトにおける不具合について Oxalyl chloride MSDS sold here are of the highest quality used in oxidation... Or water Materials Strong oxidizing agents Hazardous Decomposition ProductsCarbon monoxide ( CO,. Of water for at least 15 minutes the reagent degrades into volatile side products in this application which... Milder, more selective reagent a useful reagent in organic synthesis, N-dimethylformamide catalyzed reaction is a useful reagent organic. The Vilsmeier–Haack reaction from ethylene carbonate corresponding acyl choride using aluminum chloride as.... On clothing ( ご提供している分析チャートの種類は製品ごとに異なります。 ) ｜ tciメール最新号no.185を公開しました。 ｜ 弊社ウェブサイトにおける不具合について Oxalyl chloride for.... And ketones cas 79-37-8, EC Number 201-200-2, chemical formula ClCOCOCl a catalyst in the first stage the...
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